HCID 46736955, compound → HCID 90407152, compound

HRID 2277505Notes

Reaction equation

HRID 2277505 reaction equation
[NH:1]1[CH:5]=[C:4]([C:6]2[CH:11]=[C:10]([C:12]#[N:13])[CH:9]=[CH:8][N:7]=2)[N:3]=[CH:2]1.Cl.Cl[CH2:16][CH:17]([N:19]1[CH2:23][CH2:22][CH2:21][CH2:20]1)[CH3:18]>>[N:19]1([CH:17]([CH3:18])[CH2:16][N:1]2[CH:5]=[C:4]([C:6]3[CH:11]=[C:10]([C:12]#[N:13])[CH:9]=[CH:8][N:7]=3)[N:3]=[CH:2]2)[CH2:23][CH2:22][CH2:21][CH2:20]1

Participants

3

Reactant 2

HCID 46736955HCID 46736955, compoundHCID 178510201HCID 178510201, compound

Product 1

HCID 90407152HCID 90407152, compound

Procedure

The title compound was prepared from 2-(1H-imidazol-4-yl)pyridine-4-carbonitrile and 1-(2-chloro-1-methylethyl)pyrrolidine hydrogen chloride according to the procedure for the preparation of Example 43, part A (heating to 120°). [M+H] Calc'd for C16H19N5, 282. Found, 282.

Workup

  1. temperatureA (heating to 120°)

Sources & evidence

ORD record
ord-e191c882a1744e62b2e063bf8544666c
Source dataset
uspto-grants-2015_09
Patent number
US09133166B2

Reaction notes

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