1-(Bromomethyl)-2,3-dichlorobenzene → HCID 90407359, compound

HRID 2277563Notes

Reaction equation

HRID 2277563 reaction equation
[NH:1]1[CH:5]=[C:4]([C:6]2[CH:11]=[C:10]([C:12]#[N:13])[CH:9]=[CH:8][N:7]=2)[N:3]=[CH:2]1.[Cl:14][C:15]1[C:22]([Cl:23])=[CH:21][CH:20]=[CH:19][C:16]=1[CH2:17]Br>>[Cl:14][C:15]1[C:22]([Cl:23])=[CH:21][CH:20]=[CH:19][C:16]=1[CH2:17][N:1]1[CH:5]=[C:4]([C:6]2[CH:11]=[C:10]([C:12]#[N:13])[CH:9]=[CH:8][N:7]=2)[N:3]=[CH:2]1

Participants

3

Reactant 2

HCID 27346021-(Bromomethyl)-2,3-dichlorobenzeneHCID 178510201HCID 178510201, compound

Product 1

HCID 90407359HCID 90407359, compound

Procedure

The title compound was prepared from 2-(1H-imidazol-4-yl)pyridine-4-carbonitrile (PREPARATION 4) and 2,3-dichlorobenzylbromide according to the procedure for the preparation of Example 43, part A using room temp. [M+H] Calc'd for C16H10Cl2N4, 330. Found, 330.

Sources & evidence

ORD record
ord-6fc3fca96eb840009ad20ab2bfc4722b
Source dataset
uspto-grants-2015_09
Patent number
US09133166B2

Reaction notes

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