1H-1,2,4-Triazole → HCID 86685952, compound

HRID 2277643Notes

Reaction equation

HRID 2277643 reaction equation
[NH:1]1[CH:5]=[N:4][CH:3]=[N:2]1.[Br:6][C:7]1[CH:8]=[N:9][CH:10]=[C:11]([CH2:13]Cl)[CH:12]=1>>[Br:6][C:7]1[CH:8]=[N:9][CH:10]=[C:11]([CH2:13][N:1]2[CH:5]=[N:4][CH:3]=[N:2]2)[CH:12]=1

Participants

3

Reactant 2

HCID 92571H-1,2,4-TriazoleHCID 117012593-Bromo-5-(chloromethyl)pyridine

Product 1

HCID 86685952HCID 86685952, compound

Procedure

In analogy to the procedure described for the preparation of intermediates B-1 [B], 1H-1,2,4-triazole has been coupled to 3-bromo-5-chloromethyl-pyridine (intermediate B-1 [A]) to yield the title compound as a white solid. MS: 238.9, 241.3 (M+H+).

Sources & evidence

ORD record
ord-8625cb5c8ad44edf98607405a5c648a2
Source dataset
uspto-grants-2015_09
Patent number
US09133158B2

Reaction notes

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