HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2',4'-Dichloro-biphenyl-4-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2',4'-Dichloro-biphenyl-4-carboxylic acid | HCID 10754279 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2',4'-Dichloro-biphenyl-4-carbonyl chloride | HCID 57757250 | — |
Reaction Steps
2′,4′-Dichloro-biphenyl-4-carboxylic acid (2 g) was suspended in toluene (30 mL) and thionyl chloride (5 mL) added. The mixture was heated to reflux for 4 hours and then evaporated to dryness and the procedure repeated. Evaporation gave the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07560597B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-e8293bd9c52e4ff0998120728b27fb20 |
| Source note | uspto-grants-2009_07 |