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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2279262Generated: October 30, 2026

Hydrochloric Acid → HCID 86697003, compound

https://huagongshe.com/reaction/2279262

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 86697004HCID 86697004—
SolventDichloromethaneHCID 6344—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 86697003HCID 86697003120.1%

Reaction Steps

To a solution of compound 91 (1613 mg, 4.826 mmol) in DCM (10 ml) was added 4N HCl in dioxane.(10 ml). The solution was allowed to stir at room temperature for 2 hours, then the reaction mixture was concentrated to give compound 196 (1357 mg, 104%) as a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09133215B2
Source datasetuspto-grants-2015_09
ORD IDord-3b09a2addd304796827298e2b928baa5
Source noteuspto-grants-2015_09