HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetamidobenzaldehyde → N-[4-(8-benzyloxy-3-cyclohexylaminoimidazo[1,2-a]pyridin-2-yl)-phenyl]-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetamidobenzaldehyde | HCID 73942 | — |
| Reactant | Cyclohexyl isocyanide | HCID 79129 | — |
| Reactant | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | N-[4-(8-benzyloxy-3-cyclohexylaminoimidazo[1,2-a]pyridin-2-yl)-phenyl]-acetamide | HCID 9911805 | — |
Reaction Steps
Compound (7) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3-benzyloxypyridine solution (0.1 M, DCM), 0.575 ml of cyclohexyl isocyanide solution (0.2 M, DCM), 0.500 ml of 4-acetamidobenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849642B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-f941adf25dc84ba8b696c02443532c05 |
| Source note | uspto-grants-2005_02 |