Dichloromethane → HCID 60198594, compound

Participants

Reaction Steps

To a solution of 268 (0.075 g, 0.14 mmol) and DCM (3 mL) at RT was added TFA (2 mL) and the reaction was stirred at RT for 1 h then concentrated to dryness. The resulting product was next dissolved in minimal DCM (with MeOH to increase solubility) and added with stirring to a solution of 1M HCl in ether. The resulting solid was filtered, washed with ether and dried to afford 0.050 g (75%) of I-66: MS m/z (APCI-pos) M+1=455.

Provenance & Evidence