Dichloromethane → HCID 60198721, compound

Participants

Reaction Steps

To a solution of 318 (0.100 g, 0.175 mmol) and DCM (5 mL) at RT was added TFA (2 mL) and the reaction was stirred at RT for 1 h then concentrated to dryness. The crude product was next dissolved in minimal DCM (with MeOH to aid solubility) and added to a stirred solution of 1M HCl in ether. The resulting solid was filtered, washed with ether and dried to afford 0.070 g (78.8%) of I-80: MS m/z (APCI-pos) M+1=471.

Provenance & Evidence