HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxybenzaldehyde → Cyclohexyl-[6,8-dibromo-2-(2-methoxyphenyl)-5-methyl-imidazo[1,2-a]pyridin-3-yl]-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxybenzaldehyde | HCID 8658 | — |
| Reactant | Cyclohexyl isocyanide | HCID 79129 | — |
| Reactant | Wisteria sinensis, ext. | HCID 522994 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | Cyclohexyl-[6,8-dibromo-2-(2-methoxyphenyl)-5-methyl-imidazo[1,2-a]pyridin-3-yl]-amine | HCID 9891862 | — |
Reaction Steps
Compound (11) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-3,5-dibromo-6-methylpyridine solution (0.1 M, DCM), 0.575 ml of cyclohexyl isocyanide solution (0.2 M, DCM), 0.500 ml of 2-methoxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849642B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-953a04bcea68431cb7c804ceb37f0d09 |
| Source note | uspto-grants-2005_02 |