Methacrylic Acid → HCID 86707575, compound

HRID 2279969Notes

Reaction equation

[OH:1][CH2:2][CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][C:8]([C:11]2[CH:16]=[C:15]([OH:17])[CH:14]=[C:13]([C:18]3[CH:23]=[CH:22][C:21]([CH2:24][CH2:25][CH2:26][OH:27])=[CH:20][CH:19]=3)[CH:12]=2)=[CH:7][CH:6]=1.[C:28]([OH:33])(=O)[C:29]([CH3:31])=[CH2:30]>>[CH3:30][C:29](=[CH2:31])[C:28]([O:1][CH2:2][CH2:3][CH2:4][C:5]1[CH:6]=[CH:7][C:8]([C:11]2[CH:16]=[C:15]([O:17][C:28](=[O:33])[C:29]([CH3:31])=[CH2:30])[CH:14]=[C:13]([C:18]3[CH:23]=[CH:22][C:21]([CH2:24][CH2:25][CH2:26][O:27][C:28](=[O:33])[C:29]([CH3:31])=[CH2:30])=[CH:20][CH:19]=3)[CH:12]=2)=[CH:9][CH:10]=1)=[O:33]

Participants

Reactant 2

HCID 4093Methacrylic Acid

HCID 86707574HCID 86707574, compound

Product 1

HCID 86707575HCID 86707575, compound

Procedure

In analogy to step 2 of example 1, 4,4″-bis-(3-hydroxy-propyl)-[1,1′;3′,1″]terphenyl-5′-ol and methacrylic acid are reacted to give 2-methyl-acrylic acid-4,4″-bis-[3-(2-methyl-acryloyloxy)-propyl]-[1,1′;3′,1″]terphenyl-5′-yl ester as colourless oil.

Sources & evidence

ORD record: ord-fbb01878ef9742128443b6bda4865e49
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09133395B2

Reaction notes

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