Methacrylic Acid → HCID 86707579, compound

HRID 2279972Notes

Reaction equation

[OH:1][CH2:2][CH2:3][CH2:4][C:5]1[CH:6]=[C:7]([C:18]2[CH:23]=[CH:22][C:21]([OH:24])=[CH:20][CH:19]=2)[CH:8]=[C:9]([C:11]2[CH:16]=[CH:15][C:14]([OH:17])=[CH:13][CH:12]=2)[CH:10]=1.[C:25]([OH:30])(=O)[C:26]([CH3:28])=[CH2:27]>>[CH3:27][C:26](=[CH2:28])[C:25]([O:24][C:21]1[CH:20]=[CH:19][C:18]([C:7]2[CH:6]=[C:5]([CH2:4][CH2:3][CH2:2][O:1][C:25](=[O:30])[C:26]([CH3:28])=[CH2:27])[CH:10]=[C:9]([C:11]3[CH:12]=[CH:13][C:14]([O:17][C:25](=[O:30])[C:26]([CH3:28])=[CH2:27])=[CH:15][CH:16]=3)[CH:8]=2)=[CH:23][CH:22]=1)=[O:30]

Participants

Reactant 2

HCID 4093Methacrylic Acid

HCID 86707577HCID 86707577, compound

Product 1

HCID 86707579HCID 86707579, compound

Procedure

In analogy to step 2 of example 1, 5′-(3-hydroxy-propyl)-[1,1′;3′,1″]terphenyl-4,4″-diol and methacrylic acid are reacted to give 2-methyl-acrylic acid-3-[4,4″-bis-(2-methyl-acryloyloxy)-[1,1′;3′,1″]terphenyl-5′-yl]-propyl ester as colourless, viscous oil.

Sources & evidence

ORD record: ord-c459159baa374fbb8e399824a2556e63
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09133395B2

Reaction notes

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