HCID 86702657, compound → HCID 86702656, compound

Participants

Reaction Conditions

Reaction Steps

To a 2-5 mL MWI vial equipped with a stir bar was added the ene-allene-yne 1 (50 mg, 0.19 mmol) in o-dichlorobenzene (2.5 mL), and the reaction was irradiated with stirring at 225° C. for 10 min until complete by TLC. The reaction was then transferred directly to a silica gel cartridge and purified by silica gel column chromatography (25 g silica cartridge, 0-3% Et2O/pentane) to yield 2 as a light yellow oil (34 mg, 68%).

Provenance & Evidence