HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → Cyclohexyl-(2,5,7-trimethylimidazo[1,2-a]pyridin-3-yl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | 2-Amino-4,6-dimethylpyridine | HCID 21507 | — |
| Reactant | Cyclohexyl isocyanide | HCID 79129 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | Cyclohexyl-(2,5,7-trimethylimidazo[1,2-a]pyridin-3-yl)-amine | HCID 9816566 | — |
Reaction Steps
Compound (19) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-4,6-dimethylpyridine solution (0.1 M, DCM), 0.575 ml of cyclohexyl isocyanide solution (0.2 M, DCM), 0.500 ml of acetaldehyde solution (0.3 M, DCM) and 10 μl of perchloric acid (w=20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849642B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-793046b5752c4850a3b36506c79c4a06 |
| Source note | uspto-grants-2005_02 |