HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4-methylpyridine → [2-(3,4-Dimethoxyphenyl)-7-methylimidazo[1,2-a]pyridin-3-yl]-(6-isocyanohexyl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4-methylpyridine | HCID 1533 | — |
| Reactant | Veratraldehyde | HCID 8419 | — |
| Reactant | 1,6-Diisocyanohexane | HCID 3391105 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | [2-(3,4-Dimethoxyphenyl)-7-methylimidazo[1,2-a]pyridin-3-yl]-(6-isocyanohexyl)-amine | HCID 22591917 | — |
Reaction Steps
Compound (24) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-4-methylpyridine solution (0.1 M, DCM), 0.575 ml of 1,6-diisocyanhexane solution (0.2 M, DCM), 0.500 ml of 3,4-dimethoxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06849642B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-69da732a5c2f44f58af76bcf57f85822 |
| Source note | uspto-grants-2005_02 |