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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2280910Generated: October 30, 2026

Phenyl dihydrogen orthoborate → Tert-butyl 4,6-dimethyl-2-(2-(methyl(1-phenylpiperidine-4-yl)amino)-2-oxoethoxy)pyrimidine-5-ylcarbamate

https://huagongshe.com/reaction/2280910

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenyl dihydrogen orthoborateHCID 78412—
ReactantTert-butyl 4,6-dimethyl-2-(2-(methyl(piperidine-4-yl)amino)-2-oxoethoxy)pyrimidine-5-ylcarbamateHCID 59336171—
CatalystCupric acetateHCID 8895—
SolventPyridineHCID 1049—
ProductTert-butyl 4,6-dimethyl-2-(2-(methyl(1-phenylpiperidine-4-yl)amino)-2-oxoethoxy)pyrimidine-5-ylcarbamateHCID 59336161—

Reaction Steps

The title compound was synthesized from Compound 31, phenylboric acid, copper (II) acetate and pyridine in the same manner as in Example 32.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09139559B2
Source datasetuspto-grants-2015_09
ORD IDord-0590a0d0821147dfb8d04af60a8f921c
Source noteuspto-grants-2015_09