Sodium Azide → HCID 86700767, compound

HRID 2280975Notes

Reaction equation

Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9].[N-:11]=[N+:12]=[N-:13].[Na+]>>[N:11]([CH:4]([CH2:3][CH3:2])[CH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9])=[N+:12]=[N-:13]

Participants

Reactant 2

HCID 33557Sodium Azide

HCID 1217237-Bromoheptanoic acid

Product 1

HCID 86700767HCID 86700767, compound

Procedure

Reaction of 7-bromoheptanoic acid and NaN3, as described for the synthesis of 6, gave 5-azidoheptanoic acid 10. Saponification was not necessary. Used without further purification.

Workup

customas described for the synthesis of 6

Sources & evidence

ORD record: ord-288d680a1c5046558bc13e4967e40760
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09139565B2

Reaction notes

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