Sodium Azide → HCID 86700768, compound

HRID 2280976Notes

Reaction equation

Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10].[N-:12]=[N+:13]=[N-:14].[Na+]>>[N:12]([CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10])=[N+:13]=[N-:14]

Participants

Reactant 2

HCID 33557Sodium Azide

HCID 5482758-Bromooctanoic acid

Product 1

HCID 86700768HCID 86700768, compound

Procedure

Reaction of 8-bromooctanoic acid and NaN3, as described for the synthesis of 6, gave 8-azidooctanoic acid 11. Saponification was not necessary. Used without further purification.

Workup

customas described for the synthesis of 6

Sources & evidence

ORD record: ord-3f839ba373c74e56af0ac4415f3ccdf7
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09139565B2

Reaction notes

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