HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Diazabicyclo(3.2.2)nonane → HCID 68328293, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Diazabicyclo(3.2.2)nonane | HCID 398407 | — |
| Reactant | HCID 17958489 | HCID 17958489 | — |
| Product | HCID 68328293 | HCID 68328293 | 15% |
Reaction Steps
Biphenyl-2-yl carbonochloridate (83.0 mg, 0.358 mmol) was treated with 1,4-diazabicyclo[3.2.2]nonane (113 mg, 0.896 mmol) using the same procedure reported in example 46 to afford the title compound as an off-white solid (17 mg, 15%). Purity: >99% UPLCMS (210 nm); retention time 0.75 min; (M+1) 323.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09139580B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-6fd1c9765e514cc392a19c26239aae04 |
| Source note | uspto-grants-2015_09 |