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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2281399Generated: November 1, 2026

HCID 86636611, compound → HCID 44467019, compound

https://huagongshe.com/reaction/2281399

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86636611HCID 86636611—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 44467019HCID 4446701967.5%

Reaction Steps

A solution of tert-butyl (1-(5-fluoro-2-(2-oxo-1,2,3,4-tetrahydroquinolin-6-ylamino)pyrimidin-4-yl)piperidin-4-yl)methylcarbamate (55 mg, 0.12 mmol) in TFA (3 mL) was stirred at room temperature for 60 min. TFA was removed in vacuo. The residue was purified by HPLC to give the titled compound (30 mg) MS 371.3 (M+H); UV 206.8, 274.8 nm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09139581B2
Source datasetuspto-grants-2015_09
ORD IDord-ceefacc9defb44499a76ae8b865ed87a
Source noteuspto-grants-2015_09