HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67086938, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 67086791 | HCID 67086791 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67086938 | HCID 67086938 | — |
Reaction Steps
To 3-(4-Methoxycarbonylmethoxy-phenyl)-propionic acid tert-butyl ester (0.097 g, 0.33 mmol) is added a 90% solution of TFA in DCM (2 ml) and the resulting solution is stirred at room temperature for 1 hour. The solvents are removed in vacuo to yield 3-(4-Methoxycarbonylmethoxy-phenyl)-propionic acid as an off-white powder; [M+H-18]+ 256.0
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09139586B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-82beb0b0783b45cfbdd38700e22f17b7 |
| Source note | uspto-grants-2015_09 |