HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 71555126, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 89523946 | HCID 89523946 | — |
| Product | HCID 71555126 | HCID 71555126 | 84% |
Reaction Steps
In analogy to the experimental procedure of example 1c) rac-3-(2,4-Dichloro-benzylcarbamoyl)-3,6-diaza-bicyclo[3.2.0]heptane instead of 6-(2,4-dichloro-benzylcarbamoyl)-2,6-diaza-spiro[3.3]heptane using benzoyl chloride was converted into the title compound (92 mg, 84%) which was obtained as a white solid. MS (EI) m/e: 404.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09139593B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-494ea0c6f97745b49f2e97b62482ec52 |
| Source note | uspto-grants-2015_09 |