HCID 69938093, compound → HCID 69937546, compound

Participants

Reaction Conditions

Reaction Steps

(±)-tert-Butyl ((4aS*,7aS*)-7a-(2-fluoro-5-nitrophenyl)-3-methyl-4-oxo-3,4,4a,5,7,7a-hexahydrofuro[3,4-d]pyrimidin-2-yl)carbamate (60 mg, 0.14 mmol) was transferred into the reaction vessel. Zinc (100 mg, 1.53 mmol) was transferred into the reaction vessel. The reaction was stirred at 0° C. for 30 mins. The reaction was filtered, concentrated and the residue was purified by flash chromatography (EtOAc/Hexane, 20-100%) to give the title compound (56 mg). LCMS (Method A) Rt 2.33 min, ESI-MS: m/z 279 [MH-BOC]+.

Provenance & Evidence