Methanesulfonyl chloride → HCID 541904, compound

HRID 2281960Notes

Reaction equation

C(O[C:6]([N:8](C)[CH2:9][CH2:10][NH2:11])=O)(C)(C)C.[CH3:13][S:14](Cl)(=[O:16])=[O:15]>>[CH3:6][NH:8][CH2:9][CH2:10][NH:11][S:14]([CH3:13])(=[O:16])=[O:15]

Participants

Reactant 2

HCID 31297Methanesulfonyl chloride

HCID 2756424N-Boc-N-methylethylenediamine

Product 1

HCID 541904HCID 541904, compound

Procedure

By using N-t-butoxycarbonyl-N-methylethylenediamine (500 mg) and methanesulfonyl chloride (289 μl) as starting materials, the title compound (260 mg) was obtained in the same manner as that of Reference Example 58.

Sources & evidence

ORD record: ord-545828abfa734bfea1e8534fea25c550
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09139609B2

Reaction notes

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