p-Toluenesulfonic acid monohydrate → HCID 178427644, compound

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Reaction Steps

The title compound has been prepared according to the similar manner described in 85-B (iv) from 5-[2-(4,4-difluoropiperidin-1-yl)ethoxy]-2-methyl-3-[4-phenyl-5-(1H-1,2,4-triazol-3-yl)-1,3-thiazol-2-yl]pyrazolo[1,5-a]pyridine (87.8 mg, 0.168 mmol) and p-toluenesulfonic acid monohydrate (70.3 mg, 0.370 mmol). The crude product was washed with EtOH (4 mL) to give pure title compound (100 mg, 69%) as a yellow solid.

Provenance & Evidence