HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 59770826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 86684648 | HCID 86684648 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 59770826 | HCID 59770826 | — |
Reaction Steps
1 g of 9,9′-(5-(trimethylsilyl)-1,3-phenylene)bis(9H-carbazole) and 0.40 g of N-bromosuccinimide were dissolved in 20 mL of dimethylformamide, and then the reaction was carried out at room temperature. After completion of the reaction, the reaction mixture was extracted with dichloromethane and distilled water, and the solvent was dried. The resulting solid was filtered and purified, yielding 9,9′-(5-bromo-1,3-phenylene)bis(9H-carbazole) as an intermediate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09142784B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-b73746c9cb0c4256b59898df5b7068b6 |
| Source note | uspto-grants-2015_09 |