Potassium Carbonate → HCID 86684649, compound

Participants

Reaction Conditions

Reaction Steps

1.00 g of 9,9′-(5-bromo-1,3-phenylene)bis(9H-carbazole), 0.65 g of 3-bromo-9H-carbazole, 1.13 g of potassium carbonate, 0.26 g of copper powder and 0.05 g of dibenzo-18-crown-6 were dissolved in 20 mL of o-dichlorobenzene, and the resulting solution was refluxed at a steady 100° C. After completion of the reaction, the reaction mixture was extracted with dichloromethane and distilled water, and the solvent was dried. The resulting solid was filtered and purified, yielding 9,9′-(5-(3-bromo-9H-carbazol-9-yl)-1,3-phenylene)bis(9H-carbazole) as an intermediate.

Provenance & Evidence