HuagongsheHuagongshe Chemistry Print Report · For research reference only
((4-Bromobutoxy)methyl)benzene → HCID 11526669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ((4-Bromobutoxy)methyl)benzene | HCID 4422181 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11526669 | HCID 11526669 | 48.3% |
Reaction Steps
Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0646 g, 0.220 mmol) and 4-bromobutyl phenylmethyl ether (0.090 mL, 0.472 mmol) in 2 CH3CN/3 CHCl3 (5.0 mL) were reacted to give the desired product (0.0531 g, 48.3%). EI-MS m/z 456 (M+) Rt (2.09 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09144571B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-cdcd041a37ca457e8f45d281d0437231 |
| Source note | uspto-grants-2015_09 |