HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Bromide → HCID 11545844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11545844 | HCID 11545844 | 54.9% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0581 g, 0.198 mmol) and bromoethane (0.030 mL, 0.402 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0434 g, 54.9%). EI-MS m/z 322 (M+) Rt (1.56 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09144571B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-b8e6a7c049494a71a1d18edca5ee38e7 |
| Source note | uspto-grants-2015_09 |