HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pentene, 5-bromo- → HCID 11539496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pentene, 5-bromo- | HCID 70704 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11539496 | HCID 11539496 | 88.6% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0608 g, 0.207 mmol) and 5-bromo-1-pentene (0.045 mL, 0.380 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0806 g, 88.6%). EI-MS m/z 362 (M+) Rt (1.88 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09144571B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-f0ad8afdd7da421c9dd75d4ad1dc109e |
| Source note | uspto-grants-2015_09 |