HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-3-Bromopropylphthalimide → HCID 68959633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-3-Bromopropylphthalimide | HCID 21611 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 68959633 | HCID 68959633 | 82.4% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0861 g, 0.293 mmol) and 2-(3-bromopropyl)-1H-isoindole-1,3(2H)-dione (0.118 g, 0.440 mmol) in 2 CH3CN/3 CHCl3 (5.0 mL) were reacted to give the desired product (0.1319 g, 82.4%). EI-MS m/z 481 (M+) Rt (1.90 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09144571B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-91f8eacd3dab45d89540e52910fc56f5 |
| Source note | uspto-grants-2015_09 |