HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-bromo-2-(3-bromopropoxy)benzene → HCID 11497979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-bromo-2-(3-bromopropoxy)benzene | HCID 334092 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11497979 | HCID 11497979 | 74.8% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0472 g, 0.161 mmol) and 2-bromophenyl 3-bromopropyl ether (0.0648 g, 0.220 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0703 g, 74.8%). EI-MS m/z 507 (M+) Rt (2.18 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09144571B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-e4860a50d7a94211a1a1949a6ada44a7 |
| Source note | uspto-grants-2015_09 |