HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 67178891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 4-Heptylphenol | HCID 16143 | — |
| Product | HCID 67178891 | HCID 67178891 | 78% |
Reaction Steps
The same method as step (6-1) of Example 6 was carried out with the exception of using 14629 g of p-heptyl phenol instead of 4-phenyl phenol, using 959 g of urea and carrying out the reaction for 17 hours. When a portion of the reaction liquid was removed and analyzed by liquid chromatography, the formation of (p-heptylphenyl) carbamate was confirmed. The yield was about 78% based on the charged amount of urea.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145357B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-aa77d274efc2412dacbfad728f5d0dcf |
| Source note | uspto-grants-2015_09 |