HCID 42644137, compound → HCID 57751092, compound

Participants

Reaction Steps

(E)-2-(2-(2-Methoxyphenyl)vinylsulfonamido)benzenesulfonamide (94 mg, 0.26 mmol) was dissolved in methanol (5 mL) in a 5 mL syringe. The solution was injected to the H-cube (1 ml/min, full hydrogen; 10% Pd/C). The solvent was then removed under reduced pressure and the crude material was purified by preparative HPLC (XTerra MS C8 column, acetonitrile/ammonium acetate buffer) to give the title compound (69 mg, 73%).

Provenance & Evidence