3,3-Dimethyl-1-butyne → HCID 57751080, compound

HRID 2283321Notes

Reaction equation

HRID 2283321 reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][S:10]([NH:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2[S:20]([NH2:23])(=[O:22])=[O:21])(=[O:12])=[O:11])=[CH:4][CH:3]=1.[CH3:24][C:25]([CH3:29])([CH3:28])[C:26]#[CH:27]>>[CH3:24][C:25]([CH3:29])([CH3:28])[C:26]#[C:27][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][S:10]([NH:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2[S:20]([NH2:23])(=[O:22])=[O:21])(=[O:12])=[O:11])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 135123,3-Dimethyl-1-butyneHCID 57750969HCID 57750969, compound

Product 1

HCID 57751080HCID 57751080, compoundYield 16%

Procedure

The title compound was synthesized as described for Example 179a) in 16% yield, starting from 2-(2-(4-bromophenyl)ethylsulfonamido)benzenesulfonamide and 3,3-dimethyl-1-butyne.

Sources & evidence

ORD record
ord-9b7851792e364eb082d646578978ceaf
Source dataset
uspto-grants-2015_09
Patent number
US09145380B2

Reaction notes

Loading…