2-Aminobenzenesulfonamide → HCID 57751054, compound

HRID 2283331Notes

Reaction equation

[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[S:8]([NH2:11])(=[O:10])=[O:9].[CH3:12][C:13]1[S:14][CH:15]=[C:16]([C:18]2[CH:19]=[C:20]([S:24](Cl)(=[O:26])=[O:25])[CH:21]=[CH:22][CH:23]=2)[N:17]=1>>[CH3:12][C:13]1[S:14][CH:15]=[C:16]([C:18]2[CH:19]=[C:20]([S:24]([NH:1][C:2]3[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=3[S:8](=[O:9])(=[O:10])[NH2:11])(=[O:26])=[O:25])[CH:21]=[CH:22][CH:23]=2)[N:17]=1

Participants

Reactant 2

HCID 728942-Aminobenzenesulfonamide

HCID 155609153-(2-Methyl-1,3-thiazol-4-yl)benzene-1-sulfonyl chloride

Product 1

HCID 57751054HCID 57751054, compoundYield 5%

Procedure

The title compound was synthesized as described for Example 178 in 5% yield, starting from 2-aminobenzenesulfonamide and 3-(2-methylthiazol-4-yl)benzene-1-sulfonyl chloride.

Sources & evidence

ORD record: ord-10171edccfdc4e73802937ea8697630d
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09145380B2

Reaction notes

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