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HRID2283339

反应详情

EQUATION

反应方程式

HRID 2283339 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(N)(=O)=O)c(N)c1
HCID11436538

2-amino-4-methylbenzenesulfonamide

C7H10N2O2S

结构：O=S(=O)(Cl)/C=C/c1ccc(Cl)c(Cl)c1
HCID22719686

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(S(N)(=O)=O)c(NS(=O)(=O)/C=C/c2ccc(Cl)c(Cl)c2)c1
HCID57751111

未命名化合物

收率 54%

PROCEDURE

实验过程

The title compound was synthesized as described for Example 194 a) in 54% yield, starting from 2-amino-4-methylbenzenesulfonamide and (E)-2-(3,4-dichlorophenyl)ethenesulfonyl chloride (1.5 equiv.). Purification by column chromatography, using chloroform/methanol (95:5) as the eluent.

WORKUP

后处理

  1. customPurification by column chromatography