huagongshe.com
HRID2283349

反应详情

EQUATION

反应方程式

HRID 2283349 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(Cl)ccc1/C=C/S(=O)(=O)Cl
HCID22711054

未命名化合物

结构：C=CCN(CC=C)S(=O)(=O)c1cnccc1N
HCID57750998

未命名化合物

PRODUCTS

生成物

1
结构：C=CCN(CC=C)S(=O)(=O)c1cnccc1NS(=O)(=O)/C=C/c1ccc(Cl)cc1OC
HCID57750940

未命名化合物

收率 50%

PROCEDURE

实验过程

The title compound was synthesized as described for Example 204 c) in 50% yield, starting from N,N-diallyl-4-aminopyridine-3-sulfonamide and (E)-2-(4-chloro-2-methoxyphenyl)ethenesulfonyl chloride. Purification by column chromatography, using chloroform/methanol (98:2) as the eluent.

WORKUP

后处理

  1. customPurification by column chromatography