HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 1-Ethyl-1H-benzoimidazol-5-ylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | 5-Nitrobenzimidazole | HCID 7195 | — |
| Reactant | HCID 90308836 | HCID 90308836 | — |
| Product | 1-Ethyl-1H-benzoimidazol-5-ylamine | HCID 1507595 | — |
Reaction Steps
In accordance with Example 68 (Step 2), 5-nitrobenzoimidazole was used instead of 4-nitro-1H-indole, and iodoethane was used instead of (S)-tetrahydrofuran-3-yl methanesulfonate to obtain 1-ethyl-1H-benzo[d]imidazol-5-amine (317 mg) and 1-ethyl-1H-benzo[d]imidazol-6-amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09145414B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-61fe781a81f2418aac41b4638923355b |
| Source note | uspto-grants-2015_09 |