1H-1,3-benzodiazole-5-carbaldehyde → HCID 178482808, compound

HRID 2284110Notes

Reaction equation

HRID 2284110 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:19]=[CH:20][C:21]=1[N+:22]([O-])=O)[NH:7][C:8](=[O:18])[C:9]1[CH:14]=[CH:13][C:12]([N:15]([CH3:17])[CH3:16])=[CH:11][CH:10]=1)([O-])=O.[N:25]1[C:29]2[CH:30]=[CH:31][C:32]([CH:34]=O)=[CH:33][C:28]=2[NH:27][CH:26]=1>>[NH:22]1[C:21]2[CH:20]=[CH:19][C:6]([NH:7][C:8](=[O:18])[C:9]3[CH:14]=[CH:13][C:12]([N:15]([CH3:17])[CH3:16])=[CH:11][CH:10]=3)=[CH:5][C:4]=2[N:1]=[C:34]1[C:32]1[CH:31]=[CH:30][C:29]2[NH:25][CH:26]=[N:27][C:28]=2[CH:33]=1

Participants

3

Reactant 2

HCID 100120381H-1,3-benzodiazole-5-carbaldehydeHCID 86673952HCID 86673952, compound

Product 1

HCID 178482808HCID 178482808, compound

Procedure

Compound 187 was prepared according to the procedure similar to that described in Scheme III from 3,4-dinitro-N-(4-dimethylaminobenzoyl)aniline and benzimidazole-5-carboxaldehyde. [M+H]+ calcd for C23H20N6O: 397.17; found: 397.52.

Sources & evidence

ORD record
ord-f572efe3c6f04f508b428e2f96b58792
Source dataset
uspto-grants-2015_09
Patent number
US09144557B2

Reaction notes

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