HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylamino)Benzaldehyde → 4-(dimethylamino)-N-(2-(4-(dimethylamino)phenyl)-1H-benzo[d]imidazol-5-yl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylamino)Benzaldehyde | HCID 7479 | — |
| Reactant | HCID 86673952 | HCID 86673952 | — |
| Product | 4-(dimethylamino)-N-(2-(4-(dimethylamino)phenyl)-1H-benzo[d]imidazol-5-yl)benzamide | HCID 178482813 | — |
Reaction Steps
Compound 206 was prepared according to the procedure similar to that described in Scheme III from 3,4-dinitro-N-(4-dimethylaminobenzoyl)aniline and 4-dimethylaminobenzaldehyde. 1H NMR (300 MHz, DMSO-d6) δ 10.20 (s, 1H), 8.39 (s, 1H), 8.11 (d, J=8 Hz, 2H), 7.90 (d, J=9 Hz, 2H), 7.81 (d, J=9 Hz, 2H), 7.68 (d, J=9 Hz, 2H), 6.95 (d, J=9 Hz, 2H), 6.78 (d, J=9 Hz, 2H), 3.07 (s, 6H), 2.99 (s, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09144557B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-b88550e136ae4977a68c6863046f6976 |
| Source note | uspto-grants-2015_09 |