4-(Dimethylamino)Benzaldehyde → HCID 178482661, compound

HRID 2284122Notes

Reaction equation

HRID 2284122 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:16]=[CH:17][C:18]=1[N+:19]([O-])=O)[NH:7][C:8]([C:10]1[CH:15]=[CH:14][N:13]=[CH:12][CH:11]=1)=[O:9])([O-])=O.[CH3:22][N:23]([CH3:32])[C:24]1[CH:31]=[CH:30][C:27]([CH:28]=O)=[CH:26][CH:25]=1>>[CH3:22][N:23]([CH3:32])[C:24]1[CH:31]=[CH:30][C:27]([C:28]2[NH:19][C:18]3[CH:17]=[CH:16][C:6]([NH:7][C:8](=[O:9])[C:10]4[CH:15]=[CH:14][N:13]=[CH:12][CH:11]=4)=[CH:5][C:4]=3[N:1]=2)=[CH:26][CH:25]=1

Participants

3

Reactant 2

HCID 74794-(Dimethylamino)BenzaldehydeHCID 86673962HCID 86673962, compound

Product 1

HCID 178482661HCID 178482661, compound

Procedure

Compound 207 was prepared according to the procedure similar to that described in Scheme III from 3,4-dinitro-N-(pyridin-4-oyl)aniline and 4-dimethylaminobenzaldehyde. 1H NMR (500 MHz, DMSO-d6) δ 10.90 (s, 1H), 8.83 (d, J=6 Hz, 2H), 8.40 (s, 1H), 8.10 (d, J=9 Hz, 2H), 7.98 (d, J=6 Hz, 2H), 7.81 (dd, J=2, 9 Hz, 1H), 7.75 (d, J=9 Hz, 1H), 6.97 (d, J=9 Hz, 2H), 3.09 (s, 6H).

Sources & evidence

ORD record
ord-46446f9977da4e1d9c075c47b24e7840
Source dataset
uspto-grants-2015_09
Patent number
US09144557B2

Reaction notes

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