Benzaldehyde, 3-(2-hydroxyethoxy)- → HCID 178482812, compound

HRID 2284134Notes

Reaction equation

HRID 2284134 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([NH:13][C:14](=[O:24])[C:15]2[CH:20]=[CH:19][C:18]([N:21]([CH3:23])[CH3:22])=[CH:17][CH:16]=2)[CH:7]=[CH:8][C:9]=1[N+:10]([O-])=O)([O-])=O.[OH:25][CH2:26][CH2:27][O:28][C:29]1[CH:30]=[C:31]([CH:34]=[CH:35][CH:36]=1)[CH:32]=O>>[CH3:22][N:21]([CH3:23])[C:18]1[CH:19]=[CH:20][C:15]([C:14]([NH:13][C:6]2[CH:7]=[CH:8][C:9]3[NH:10][C:32]([C:31]4[CH:34]=[CH:35][CH:36]=[C:29]([O:28][CH2:27][CH2:26][OH:25])[CH:30]=4)=[N:1][C:4]=3[CH:5]=2)=[O:24])=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 6453965Benzaldehyde, 3-(2-hydroxyethoxy)-HCID 86673952HCID 86673952, compound

Product 1

HCID 178482812HCID 178482812, compound

Procedure

Compound 219 was prepared according to the procedure similar to that described in Scheme III from N-(3,4-dinitrophenyl)-4-dimethylaminobenzamide and 3-(2-hydroxyethyloxy)benzaldehyde. [M+H]+ calcd for C24H24N4O3: 417.19; found: 416.94.

Sources & evidence

ORD record
ord-cc65a228452a46639e44c62fea8671df
Source dataset
uspto-grants-2015_09
Patent number
US09144557B2

Reaction notes

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