Benzaldehyde, 4-(2-hydroxyethoxy)- → HCID 178484446, compound

HRID 2284137Notes

Reaction equation

HRID 2284137 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([NH:13][C:14](=[O:26])[C:15]2[CH:20]=[CH:19][C:18]([N:21]([CH3:25])[CH2:22][CH2:23][OH:24])=[CH:17][CH:16]=2)[CH:7]=[CH:8][C:9]=1[N+:10]([O-])=O)([O-])=O.[OH:27][CH2:28][CH2:29][O:30][C:31]1[CH:38]=[CH:37][C:34]([CH:35]=O)=[CH:33][CH:32]=1>>[OH:27][CH2:28][CH2:29][O:30][C:31]1[CH:38]=[CH:37][C:34]([C:35]2[NH:10][C:9]3[CH:8]=[CH:7][C:6]([NH:13][C:14](=[O:26])[C:15]4[CH:20]=[CH:19][C:18]([N:21]([CH2:22][CH2:23][OH:24])[CH3:25])=[CH:17][CH:16]=4)=[CH:5][C:4]=3[N:1]=2)=[CH:33][CH:32]=1

Participants

3

Reactant 2

HCID 89178Benzaldehyde, 4-(2-hydroxyethoxy)-HCID 86673967N-(3,4-dinitrophenyl)-4-(N-2-hydroxyethyl-N-methylamino)benzamide

Product 1

HCID 178484446HCID 178484446, compound

Procedure

Compound 223 was prepared according to the procedure similar to that described in Scheme III from N-(3,4-dinitrophenyl)-4-(N-methyl-N-2-hydroxyethylamino)benzamide and 4-(2-hydroxyethyloxy)benzaldehyde. [M+H]+ calcd for C25H26N4O4: 447.21; found: 446.89.

Sources & evidence

ORD record
ord-54bc0c8d16074f96949f2bee37c6c2b2
Source dataset
uspto-grants-2015_09
Patent number
US09144557B2

Reaction notes

Loading…