4-Hydrazinylcarbonylbenzaldehyde → HCID 178514417, compound

HRID 2284142Notes

Reaction equation

[N+:1]([C:4]1[CH:5]=[C:6]([NH:13][C:14](=[O:26])[C:15]2[CH:20]=[CH:19][C:18]([N:21]3[CH2:25][CH2:24][CH2:23][CH2:22]3)=[CH:17][CH:16]=2)[CH:7]=[CH:8][C:9]=1[N+:10]([O-])=O)([O-])=O.[NH:27]([C:29]([C:31]1[CH:38]=[CH:37][C:34]([CH:35]=O)=[CH:33][CH:32]=1)=[O:30])[NH2:28]>>[NH:27]([C:29]([C:31]1[CH:38]=[CH:37][C:34]([C:35]2[NH:10][C:9]3[CH:8]=[CH:7][C:6]([NH:13][C:14](=[O:26])[C:15]4[CH:20]=[CH:19][C:18]([N:21]5[CH2:25][CH2:24][CH2:23][CH2:22]5)=[CH:17][CH:16]=4)=[CH:5][C:4]=3[N:1]=2)=[CH:33][CH:32]=1)=[O:30])[NH2:28]

Participants

Reactant 2

HCID 193679934-Hydrazinylcarbonylbenzaldehyde

HCID 86673966N-(3,4-dinitrophenyl)-4-pyrrolidinylbenzamide

Product 1

HCID 178514417HCID 178514417, compound

Procedure

Compound 230 was prepared according to the procedure similar to that described in Scheme III from N-(3,4-dinitrophenyl)-4-pyrrolidinylbenzamide and 4-hydrazinylcarbonylbenzaldehyde. [M+H]+ calcd for C25H24N6O2: 441.21; found: 441.51.

Sources & evidence

ORD record: ord-05d060d77cb54293b7a04e8d26816ae8
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09144557B2

Reaction notes

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