3,3'-Diaminobenzidine → HCID 178490007, compound

HRID 2284160Notes

Reaction equation

HRID 2284160 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([C:9]2[CH:15]=[CH:14][C:12]([NH2:13])=[C:11]([NH2:16])[CH:10]=2)[CH:5]=[CH:6][C:7]=1[NH2:8].[CH3:17][O:18][C:19]1[CH:24]=[CH:23][C:22]([CH:25]=[CH:26][CH:27]=O)=[CH:21][CH:20]=1>>[CH3:17][O:18][C:19]1[CH:24]=[CH:23][C:22](/[CH:25]=[CH:26]/[C:27]2[NH:8][C:7]3[CH:6]=[CH:5][C:4]([C:9]4[CH:15]=[CH:14][C:12]5[N:13]=[C:27](/[CH:26]=[CH:25]/[C:22]6[CH:21]=[CH:20][C:19]([O:18][CH3:17])=[CH:24][CH:23]=6)[NH:16][C:11]=5[CH:10]=4)=[CH:3][C:2]=3[N:1]=2)=[CH:21][CH:20]=1

Participants

3

Reactant 2

HCID 70713,3'-DiaminobenzidineHCID 2309953-(4-Methoxyphenyl)prop-2-enal

Product 1

HCID 178490007HCID 178490007, compound

Procedure

Compound 262 was prepared according to the procedure similar to that described in Scheme III from 3,3′-diaminobenzidine and 3-(4-methoxyphenyl)acrylaldehyde. [M+H]+ calcd for C32H26N4O2: 499.21; found: 499.00.

Sources & evidence

ORD record
ord-fa47a4cc620845bd9616fa833f0aa1b6
Source dataset
uspto-grants-2015_09
Patent number
US09144557B2

Reaction notes

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