3,3'-Diaminobenzidine → HCID 178482753, compound

HRID 2284161Notes

Reaction equation

HRID 2284161 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([C:9]2[CH:15]=[CH:14][C:12]([NH2:13])=[C:11]([NH2:16])[CH:10]=2)[CH:5]=[CH:6][C:7]=1[NH2:8].[CH3:17][N:18]([CH3:29])[C:19]1[CH:24]=[CH:23][C:22]([CH:25]=[CH:26][CH:27]=O)=[CH:21][CH:20]=1>>[NH:8]1[C:7]2[CH:6]=[CH:5][C:4]([C:9]3[CH:15]=[CH:14][C:12]4[N:13]=[C:27](/[CH:26]=[CH:25]/[C:22]5[CH:23]=[CH:24][C:19]([N:18]([CH3:29])[CH3:17])=[CH:20][CH:21]=5)[NH:16][C:11]=4[CH:10]=3)=[CH:3][C:2]=2[N:1]=[C:27]1/[CH:26]=[CH:25]/[C:22]1[CH:21]=[CH:20][C:19]([N:18]([CH3:17])[CH3:29])=[CH:24][CH:23]=1

Participants

3

Reactant 2

HCID 70713,3'-DiaminobenzidineHCID 922244-(Dimethylamino)-cinnamaldehyde

Product 1

HCID 178482753HCID 178482753, compound

Procedure

Compound 264 was prepared according to the procedure similar to that described in Scheme III from 3,3′-diaminobenzidine and 3-(4-dimethylaminophenyl)acrylaldehyde. [M+H]+ calcd for C34H32N6: 525.27; found: 525.59.

Sources & evidence

ORD record
ord-5256a00cff5c4ee89eaf09deba527bf8
Source dataset
uspto-grants-2015_09
Patent number
US09144557B2

Reaction notes

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