3,3'-Diaminobenzidine → HCID 136352327, compound

HRID 2284162Notes

Reaction equation

HRID 2284162 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([C:9]2[CH:15]=[CH:14][C:12]([NH2:13])=[C:11]([NH2:16])[CH:10]=2)[CH:5]=[CH:6][C:7]=1[NH2:8].[CH3:17][N:18]([CH3:36])[C:19]1[CH:35]=[CH:34][C:22]([C:23]([NH:25][C:26]2[CH:33]=[CH:32][C:29]([CH:30]=O)=[CH:28][CH:27]=2)=[O:24])=[CH:21][CH:20]=1>>[NH:8]1[C:7]2[CH:6]=[CH:5][C:4]([C:9]3[CH:15]=[CH:14][C:12]4[N:13]=[C:30]([C:29]5[CH:32]=[CH:33][C:26]([NH:25][C:23](=[O:24])[C:22]6[CH:34]=[CH:35][C:19]([N:18]([CH3:36])[CH3:17])=[CH:20][CH:21]=6)=[CH:27][CH:28]=5)[NH:16][C:11]=4[CH:10]=3)=[CH:3][C:2]=2[N:1]=[C:30]1[C:29]1[CH:28]=[CH:27][C:26]([NH:25][C:23](=[O:24])[C:22]2[CH:34]=[CH:35][C:19]([N:18]([CH3:36])[CH3:17])=[CH:20][CH:21]=2)=[CH:33][CH:32]=1

Participants

3

Reactant 2

HCID 70713,3'-DiaminobenzidineHCID 86673977HCID 86673977, compound

Product 1

HCID 136352327HCID 136352327, compound

Procedure

Compound 265 was prepared according to the procedure similar to that described in Scheme III from 3,3′-diaminobenzidine and 4-(4-dimethylaminobenzamido)benzaldehyde. [M+H]+ calcd for C44H38N8O2: 711.31; found: 711.38.

Sources & evidence

ORD record
ord-77939a6a0be3493ebd340b59ebcde680
Source dataset
uspto-grants-2015_09
Patent number
US09144557B2

Reaction notes

Loading…