3,3'-Diaminobenzidine → HCID 178419856, compound

HRID 2284173Notes

Reaction equation

[NH2:1][C:2]1[CH:3]=[C:4]([C:9]2[CH:15]=[CH:14][C:12]([NH2:13])=[C:11]([NH2:16])[CH:10]=2)[CH:5]=[CH:6][C:7]=1[NH2:8].[N:17]1([C:23]2[CH:30]=[CH:29][C:26]([CH:27]=O)=[CH:25][CH:24]=2)[CH2:22][CH2:21][O:20][CH2:19][CH2:18]1>>[NH:8]1[C:7]2[CH:6]=[CH:5][C:4]([C:9]3[CH:15]=[CH:14][C:12]4[N:13]=[C:27]([C:26]5[CH:29]=[CH:30][C:23]([N:17]6[CH2:22][CH2:21][O:20][CH2:19][CH2:18]6)=[CH:24][CH:25]=5)[NH:16][C:11]=4[CH:10]=3)=[CH:3][C:2]=2[N:1]=[C:27]1[C:26]1[CH:25]=[CH:24][C:23]([N:17]2[CH2:22][CH2:21][O:20][CH2:19][CH2:18]2)=[CH:30][CH:29]=1

Participants

Reactant 2

HCID 70713,3'-Diaminobenzidine

HCID 2913494-Morpholinobenzaldehyde

Product 1

HCID 178419856HCID 178419856, compound

Procedure

Compound 286 was prepared according to the procedure similar to that described in Scheme III from 3,3′-diaminobenzidine and 4-morpholinylbenzaldehyde. [M+H]+ calcd for C34H32N6O2: 557.26; found: 557.58.

Sources & evidence

ORD record: ord-ea84aeb5bf1f4ba6b07edd638befa908
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09144557B2

Reaction notes

Loading…