HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Morpholinobenzoate → N-(1-(4-Acrylamidophenyl)-1H-indazol-5-yl)-4-morpholinobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Morpholinobenzoate | HCID 5158282 | — |
| Reactant | 5-Amino-1-(4-aminophenyl)indazole | HCID 83414207 | — |
| Product | N-(1-(4-Acrylamidophenyl)-1H-indazol-5-yl)-4-morpholinobenzamide | HCID 67113416 | — |
Reaction Steps
Compound 390 was prepared according to the procedure described in Scheme IV from 5-amino-1-(4-aminophenyl)indazole and 4-morpholinobenzoate. 1H NMR (500 MHz, Acetone-d6) δ 9.59 (s, 1H), 9.47 (s, 1H), 8.49 (s, 1H), 8.24 (s, 1H), 7.98 (dd, J=2, 9 Hz, 4H), 7.81 (m, 2H), 7.77 (d, J=9 Hz, 1H), 7.05 (d, J=9 Hz, 2H), 6.52-6.38 (m, 2H), 5.75 (dd, J=2, 10 Hz, 1H), 3.80 (m, 4H), 3.29 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09144557B2 |
| Source dataset | uspto-grants-2015_09 |
| ORD ID | ord-262c481012ba41cc9f655e9c5057ba91 |
| Source note | uspto-grants-2015_09 |