Oxalic Acid → HCID 136352333, compound

HRID 2284218Notes

Reaction equation

[O:1]1[CH2:6][CH2:5][N:4]([C:7]2[CH:12]=[CH:11][C:10]([C:13]3[NH:14][C:15]4[CH:21]=[C:20]([NH2:22])[CH:19]=[CH:18][C:16]=4[N:17]=3)=[CH:9][CH:8]=2)[CH2:3][CH2:2]1.[C:23]([OH:28])(=O)[C:24](O)=[O:25]>>[O:1]1[CH2:6][CH2:5][N:4]([C:7]2[CH:12]=[CH:11][C:10]([C:13]3[NH:17][C:16]4[CH:18]=[CH:19][C:20]([NH:22][C:23](=[O:28])[C:24]([NH:22][C:20]5[CH:19]=[CH:18][C:16]6[NH:17][C:13]([C:10]7[CH:11]=[CH:12][C:7]([N:4]8[CH2:3][CH2:2][O:1][CH2:6][CH2:5]8)=[CH:8][CH:9]=7)=[N:14][C:15]=6[CH:21]=5)=[O:25])=[CH:21][C:15]=4[N:14]=3)=[CH:9][CH:8]=2)[CH2:3][CH2:2]1

Participants

Reactant 2

HCID 971Oxalic Acid

HCID 17325486HCID 17325486, compound

Product 1

HCID 136352333HCID 136352333, compound

Procedure

Compound 434 was prepared according to the procedure similar to that described in Scheme V from 2-(4-morpholinophenyl)-5-aminobenzimidazole and oxalic acid. [M+H]+ calcd for C36H34N8O4: 643.27; found: 643.09.

Sources & evidence

ORD record: ord-e194a3719e29459582b4097839ab96c5
Source dataset: uspto-grants-2015_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09144557B2

Reaction notes

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